cis-Polychloroprene was synthesized by chlorinolysis of 1,4-poly-2-(tri-n-butyltin)-l,3- butadiene. The latter was obtained by free radical polymerization of 2-(tri-n-butyltin)-l,3-butadiene. The structure of cis-polychloroprene was established by ozonolysis, and by infrared and NMR spectroscopy.

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